XRD
X-Ray Diffraction — Rigaku Smartlab SE
Capabilities and Measurements
- ›Identification of crystalline phases in solid materials (minerals, salts, synthetic compounds, etc.).
- ›Semi-quantitative estimation of crystalline phases.
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✓Submission Requirements
- Representative and correctly labeled sample.
- Dry and homogeneous material (pulverized).
- Required mass: up to 5 grams.
!Technical Limitations
- Limited sensitivity to amorphous or poorly crystalline phases.
- Approximate detection limit: 1–2 vol% (Rigaku Smartlab SE).
- Possible preferred orientation effects in certain materials.
- Requires adequate sample preparation for representative results.
- Hygroscopic or reactive materials may undergo changes during measurement (e.g., hydration).